HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20279260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 3-Pentanone, 1-chloro- | HCID 96526 | — |
| Reactant | 1-Hexylpiperazine | HCID 2736513 | — |
| Product | HCID 20279260 | HCID 20279260 | — |
Reaction Steps
A mixture of 8.5 g (0.05 mole) of a n-hexyl piperazine and 6.8 g (0.056 mole) of 1-chloro-3-pentanone was heated to 140° for 5 minutes. The reaction product was dissolved in isopropanol and acidified with a solution of HCl in isopropanol. The dihydrochloride salt was filtered and crystallized from acetonitrile to give 11.0 g of white solid with a melting point of 230°-233° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04523014 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-5eff00bce6754f48b4597b6f535d9fde |
| Source note | uspto-grants-1985_06 |