HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-bromopropionate → HCID 20279319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-bromopropionate | HCID 95576 | — |
| Reactant | HCID 20279312 | HCID 20279312 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20279319 | HCID 20279319 | — |
Reaction Steps
Methyl 2-(2-methyl-3-nitrophenoxy)propanoate (8.2 g, 40 mmole), prepared by the method of Example 1 using methyl 2-bromopropanoate, was hydrogenated in 250 ml of ethanol using 1.0 g of Raney nickel. After reduction was complete, insolubles were removed by filtration and the filtrate concentrated in vacuo. The resultant solid (7.7 g) was used in further reactions without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04523020 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-8dbec77de3cc40f2bb8eacb751846a0a |
| Source note | uspto-grants-1985_06 |