HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzoyl chloride → HCID 54275773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzoyl chloride | HCID 80172 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 5-Methoxybenzocyclobutene-1-carboxylic acid methyl ester | HCID 54118413 | — |
| Product | HCID 54275773 | HCID 54275773 | — |
Reaction Steps
In a manner analogous to that described in Example 5, starting from 26.6 g of aluminium trichloride, 9.61 g of 5-methoxybenzocyclobutene-1-carboxylic acid methyl ester and 17.56 g of p-cyanobenzoyl chloride there is obtained 4-(p-cyanobenzoyl)-5-hydroxybenzocyclobutene-1-carboxylic acid methyl ester having a melting point of 113°-114°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04523030 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-432aa8a93fb4461bba9383b98ce36a57 |
| Source note | uspto-grants-1985_06 |