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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1248405Generated: November 1, 2026

3-Pyridylmethyl-2-methylthio-4-pyrimidone → HCID 20277881, compound

https://huagongshe.com/reaction/1248405

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Pyridylmethyl-2-methylthio-4-pyrimidoneHCID 12783823—
Reactant3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamineHCID 12913950—
ProductHCID 20277881HCID 2027788156.9%

Reaction Steps

3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine (0.98 g) and 2-(methylthio)-5-[(3-pyridinyl)methyl]-4(3H)-pyrimidinone (1 g) were heated at 140° for 16 h. The residue, after column chromatography (silica/methanol -0.88 ammonia, 79:1) gave the title compound as a yellow gum (0.96 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04524071
Source datasetuspto-grants-1985_06
ORD IDord-8fe36be25c9640e59faa490077bc2f28
Source noteuspto-grants-1985_06