HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 20277870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 178494501 | HCID 178494501 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | HCID 20277870 | HCID 20277870 | 86.2% |
Reaction Steps
Dimethyl sulphate (0.363 g) was added to a stirred solution of 2-mercapto-5-[2-[3-(methoxymethyl)phenoxy]ethyl]-4(3H)-pyrimidinone (0.85 g) in water (20 ml) and potassium hydroxide (0.163 g). After 1 h., the suspension was filtered to give the title compound (0.76 g) m.p. 129°-131°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04524071 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-a66cca254b614c92a5c2582255119bc7 |
| Source note | uspto-grants-1985_06 |