反应详情

Hydrazine hydrate (28.0 mL) was dissolved in n-BuOH (200 mL) and cooled in an ice bath. A solution of 2-dimethylaminomethyl-cyclohexanone (64.0 g) in n-BuOH (50 mL) was added dropwise, the mixture was slowly warmed and refluxed for 20 hours. The solvent was evaporated under reduced pressure.

1. temperaturecooled in an ice bath
2. temperaturethe mixture was slowly warmed
3. temperaturerefluxed for 20 hours
4. customThe solvent was evaporated under reduced pressure