HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 54179722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | N-(3-acetylphenyl)propanamide | HCID 903063 | — |
| Product | HCID 54179722 | HCID 54179722 | — |
Reaction Steps
A 20 g portion of N-(3-acetylphenyl)propanamide in 50 ml of dimethylformamide dimethylacetal was refluxed for 8 hours, then evaporated. The residue was taken up in 200 ml of dichloromethane, passed through hydrous magnesium silicate, diluted with hexane and concentrated, giving 21.17 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04626538 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-647e0318f20d4f7a9fbc814b692fda3a |
| Source note | uspto-grants-1986_12 |