Benzenepropanal → HCID 70454248, compound

Participants

Reaction Steps

1.0 g (3.5 mMol) of product from Example 28 were reacted with 1.4 ml (~10 mMol) of dihydrocinnamaldehyde for 5 days in the manner described in Example 29 and, after working up by aqueous extraction, the product was chromatographed on 25 g of silica gel using toluene/ethyl acetate (4:1) and separated into the erythro and threo forms.

Provenance & Evidence