HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetic Acid → Phenylacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetic Acid | HCID 999 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Phenylacetyl chloride | HCID 7679 | — |
Reaction Steps
An amount described in Table 1 of thionyl chloride was added to an amount described in Table 1 of a derivative of phenylacetic acid and heated under reflux for one to four hours. Excess of thionyl chloride was distilled out under reduced pressure to obtain a derivative of phenylacetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04627874 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-d7829189892e4a60b11533813d67bf11 |
| Source note | uspto-grants-1986_12 |