HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 4-(3',5'-Difluorobenzyl)-3-methylthio-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 178505926 | HCID 178505926 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(3',5'-Difluorobenzyl)-3-methylthio-1,2,4-triazole | HCID 20225725 | — |
Reaction Steps
The reaction of 4-(3',5'-difluorobenzyl)-1,2,4-triazole-3-thiol (prepared as in Example 3) with methyl iodide and sodium methoxide in methanol by known techniques yields 4-(3',5'-difluorobenzyl)-3-methylthio-1,2,4-triazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628059 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-d3abad940751433185a098fa8dba367d |
| Source note | uspto-grants-1986_12 |