HRID1248957

反应详情

EQUATION

反应方程式

HRID 1248957 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

30 g of 1-formyl-2-(4-nitrophenyl)hydrazine was then catalytically reduced at room temperature in 1.6 l of ethanol using palladium-carbon as a catalyst. The reacting solution was filtered, and the filtrate was evaporated to dryness to obtain 20.5 g of 1-formyl-2-(4-aminophenyl)hydrazine as light brown solid. Melting Point: 123° to 125° C.

WORKUP

后处理

  1. filtrationThe reacting solution was filtered
  2. customthe filtrate was evaporated to dryness