HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)- → Hydrazinecarboxaldehyde, 2-(4-aminophenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)- | HCID 5008489 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Hydrazinecarboxaldehyde, 2-(4-aminophenyl)- | HCID 113189 | 81.9% |
Reaction Steps
30 g of 1-formyl-2-(4-nitrophenyl)hydrazine was then catalytically reduced at room temperature in 1.6 l of ethanol using palladium-carbon as a catalyst. The reacting solution was filtered, and the filtrate was evaporated to dryness to obtain 20.5 g of 1-formyl-2-(4-aminophenyl)hydrazine as light brown solid. Melting Point: 123° to 125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628024 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-e07bbe6995884bf798e52df4dac7dd82 |
| Source note | uspto-grants-1986_12 |