HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13374891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Butyl acetoacetate | HCID 11576 | — |
| Reactant | (2Z)-3-Amino-2-butenenitrile | HCID 5325263 | — |
| Reactant | 4-Oxo-2-phenyl-4H-1-benzothiopyran-8-carbaldehyde | HCID 13374841 | — |
| Product | HCID 13374891 | HCID 13374891 | — |
Reaction Steps
10 mmol each of 2-phenyl-4-oxo-4H-thiochromen-8-aldehyde, butyl acetoacetate and 3-aminocrotononitrile were boiled under reflux in 30 ml of ethanol overnight, the mixture was concentrated and the residue was crystallized with ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628107 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-11bdf0fae6eb4be3ab4efae1ea00a56a |
| Source note | uspto-grants-1986_12 |