HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 13561923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,2,3,4-Tetrahydro-Beta-Carboline-3-Carboxylic Acid | HCID 98285 | — |
| Product | HCID 13561923 | HCID 13561923 | — |
Reaction Steps
In the same manner as described in Example 6, (3RS)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (3.24 g), KOH (96%, 1.75 g), carbon disulfide (0.91 ml) and isopropyl iodide (1.8 ml) are reacted and treated. The product is crystallized from chloroform to give the title compound (1.59 g) as colorless needles, m.p. 188°-190° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-358e110fd96046929743a84d941a7164 |
| Source note | uspto-grants-1986_12 |