HRID1249050

反应详情

EQUATION

反应方程式

HRID 1249050 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In the same manner as descsribed in Example 32, (3S)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (4.33 g), KOH (2.33 g), carbon disulfide (1.22 ml), 50% ethanol (80 ml) and 2-thenyl chloride (3.1 g) are reacted and treated to give the title compound (3.15 g) as pale yellow powder.

WORKUP

后处理

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  2. additiontreated