HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 13561977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-(Chloromethyl)thiophene | HCID 69830 | — |
| Reactant | HCID 13562005 | HCID 13562005 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 13561977 | HCID 13561977 | — |
Reaction Steps
In the same manner as described in Example 51, (3R)-9-benzyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (1.225 g), 10N NaOH (0.8 ml), carbon disulfide (0.24 ml), dimethylsulfoxide (30 ml) and 2-thenyl chloride (0.66 g) are reacted and treated to give the title compound (0.635 g) as pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-35783251e50f4134883863c3e9c97073 |
| Source note | uspto-grants-1986_12 |