Methyl iodide → HCID 13561992, compound

Participants

Reaction Steps

In the same manner as described in Example 53, (3RS)-1,2,3,4-tetrahydro-β-carboline-3-carboxamide (0.71 g), triethylamine (0.46 ml), carbon disulfide (0.22 ml), 70% ethanol (20 ml) and methyl iodide (0.22 ml) are reacted and treated. The product is crystallized from ethyl acetate to give the title compound (0.414 g), m.p. 224°-225° C. (decomp.).

Provenance & Evidence