HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 13561994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 15573651 | HCID 15573651 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13561994 | HCID 13561994 | 71% |
Reaction Steps
In the same manner as described in Example 53, (3S)-1,2,3,4-tetrahydro-β-carboline-3-carboxamide (0.71 g), triethylamine (0.46 ml), carbon disulfide (0.22 ml), 70% ethanol (20 ml) and 4-chlorobenzyl chloride (0.53 g) are reacted and treated to give the title compound (0.97 g, 71%) as white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-d53b5744ee0e41ae9bda72a2bee2da35 |
| Source note | uspto-grants-1986_12 |