Methyl iodide → HCID 178504088, compound

Participants

Reaction Steps

In the same manner as described in Example 53, (3RS)-3-(1H-tetrazol-5-yl)-1,2,3,4-tetrahydro-β-carboline (0.257 g), triethylamine (0.23 ml), carbon disulfide (0.05 ml), 70% ethanol (4 ml) and methyl iodide (0.055 ml) are reacted and treated. The product is crystallized from chloroform to give the title compound (75 mg), m.p. 203°-205° C. (decomp.).

Provenance & Evidence