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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1249091Generated: November 3, 2026

Sodium Hydroxide → HCID 1769747, compound

https://huagongshe.com/reaction/1249091

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 40535464HCID 40535464—
SolventMethanolHCID 887—
ProductHCID 1769747HCID 1769747—

Reaction Steps

In the same manner as described in Reference Example 2-(1) using methyl (1RS,3RS)-cis-1-butyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylate (1.43 g), 1N NaOH (5.5 ml) and methanol (30 ml), there is obtained the title compound (1.06 g, 78%) as colorless needles, m.p. 215°-216° C. (recrystallized from methanol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04628057
Source datasetuspto-grants-1986_12
ORD IDord-6f66690300c04259ad46cd2f1b19b95b
Source noteuspto-grants-1986_12