HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 6997614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12789156 | HCID 12789156 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 6997614 | HCID 6997614 | 65% |
Reaction Steps
In the same manner as described in Reference Example 2-(1) using methyl (1RS,3SR)-trans-1-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylate (2.60 g), 10N NaOH (1.2 ml) and methanol (50 ml), there is obtained the title compound (1.60 g, 65%), m.p. 231°-233°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-5970c668d7054bcdbc4fd67b21347461 |
| Source note | uspto-grants-1986_12 |