Methanol → HCID 178457302, compound

HRID 1249117Notes

Reaction equation

HRID 1249117 reaction equation
[CH2:1]([NH:4][CH2:5][CH2:6][CH3:7])[CH:2]=[CH2:3].[C:8](=[S:10])=S.C[OH:12]>C(OCC)C>[CH2:1]([NH:4][CH2:5][CH2:6][CH3:7])[CH:2]=[CH2:3].[CH2:1]([N:4]([CH2:5][CH2:6][CH3:7])[C:8](=[S:10])[OH:12])[CH:2]=[CH2:3]

Participants

5

Reactant 3

HCID 887MethanolHCID 6348Carbon DisulfideHCID 123971855666-21-7

Product 1

HCID 178457302HCID 178457302, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A quantity of N-Allyl-n-propylamine (12.7 g of a 35% solution in methanol, 0.042 mole) was dissolved in 50 ml of ethyl ether, plus 1.52 g of carbon disulfide (0.02 mole) was charged into a beaker and the reaction mixture in the beaker was allowed to let stand for approximately 15 minutes, after which time the volatiles were stripped off, leaving behind 3.7 g of a solid residue, which was identified by conventional instrumental techniques as being the subject compound.

Sources & evidence

ORD record
ord-76e7aa8707fb4a9ea8f0024b9042b478
Source dataset
uspto-grants-1986_12
Patent number
US04629499

Reaction notes

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