Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1249117Generated: November 3, 2026

Methanol → HCID 178457302, compound

https://huagongshe.com/reaction/1249117

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantCarbon DisulfideHCID 6348—
ReactantAllylpropylamineHCID 12397185—
SolventDiethyl EtherHCID 3283—
ProductHCID 178457302HCID 178457302—

Reaction Steps

A quantity of N-Allyl-n-propylamine (12.7 g of a 35% solution in methanol, 0.042 mole) was dissolved in 50 ml of ethyl ether, plus 1.52 g of carbon disulfide (0.02 mole) was charged into a beaker and the reaction mixture in the beaker was allowed to let stand for approximately 15 minutes, after which time the volatiles were stripped off, leaving behind 3.7 g of a solid residue, which was identified by conventional instrumental techniques as being the subject compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04629499
Source datasetuspto-grants-1986_12
ORD IDord-76e7aa8707fb4a9ea8f0024b9042b478
Source noteuspto-grants-1986_12