Thionyl Chloride → HCID 20225301, compound

HRID 1249209Notes

Reaction equation

HRID 1249209 reaction equation
[CH3:1][O:2][CH:3](OC)[CH2:4][O:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.S(Cl)([Cl:16])=O>C(Cl)(=O)C>[Cl:16][CH:3]([O:2][CH3:1])[CH2:4][O:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 105897Benzene, (2,2-dimethoxyethoxy)-

Product 1

HCID 20225301HCID 20225301, compound

Reagents, catalysts & solvents 1

HCID 6367Acetyl chlorideSolvent

Procedure

To 36 g of phenoxyacetaldehyde dimethyl acetal was added, dropwise, 40 ml of acetyl chloride and 0.5 ml of thionyl chloride. After 15 h at room temperature the solution was evaporated and the residue distilled under vacuum, 110°-120° C./1 mm, to yield the title compound as a colourless oil.

Workup

  1. customAfter 15 h at room temperature the solution was evaporated
  2. distillationthe residue distilled under vacuum, 110°-120° C./1 mm

Sources & evidence

ORD record
ord-c44db6b523f647cc896b886c7d59af07
Source dataset
uspto-grants-1986_12
Patent number
US04629737

Reaction notes

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