HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20225301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzene, (2,2-dimethoxyethoxy)- | HCID 105897 | — |
| Solvent | Acetyl chloride | HCID 6367 | — |
| Product | HCID 20225301 | HCID 20225301 | — |
Reaction Steps
To 36 g of phenoxyacetaldehyde dimethyl acetal was added, dropwise, 40 ml of acetyl chloride and 0.5 ml of thionyl chloride. After 15 h at room temperature the solution was evaporated and the residue distilled under vacuum, 110°-120° C./1 mm, to yield the title compound as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04629737 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-c44db6b523f647cc896b886c7d59af07 |
| Source note | uspto-grants-1986_12 |