Triethylamine → HCID 882608, compound

HRID 1249226Notes

Reaction equation

HRID 1249226 reaction equation
C(N(CC)CC)C.Cl.[C:9]1([NH:15][C:16]([C:18]2[S:22][C:21]3=[N:23][CH2:24][CH2:25][N:20]3[C:19]=2[CH3:26])=[O:17])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>O>[C:9]1([NH:15][C:16]([C:18]2[S:22][C:21]3=[N:23][CH2:24][CH2:25][N:20]3[C:19]=2[CH3:26])=[O:17])[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 13192320HCID 13192320, compound

Product 1

HCID 882608HCID 882608, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Triethylamine was added to compound 2 (8.0 g, 0.027M) dissolved in water (200 ml), and the pH of the solution was adjusted to alkaline pH. The thus-formed precipitate was filtered, washed with water and dried to obtain compound 1. (70.0 g, yield: 100%).

Workup

  1. filtrationThe thus-formed precipitate was filtered
  2. washwashed with water
  3. customdried

Sources & evidence

ORD record
ord-5c4a461affec4430b9a7d26abdbd9636
Source dataset
uspto-grants-1986_12
Patent number
US04629793

Reaction notes

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