HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1249310Generated: October 28, 2026
Triphenylphosphine → HCID 178444493, compound
https://huagongshe.com/reaction/1249310
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 178444391 | HCID 178444391 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 178444493 | HCID 178444493 | 57.6% |
Reaction Steps
A mixture of 13.0 g of 1-bromo-2-(trans-4-pentylcyclohexyl)ethane, 16.0 g of triphenylphosphine and 375 ml of xylene was heated to boiling for 60 hours. After cooling to 5° C., the precipitated product was filtered off under suction, washed with toluene and hexane and dried, there being obtained 15.0 g of 2-(trans-4-pentylcyclohexyl)ethyl-triphenylphosphonium bromide; m.p. 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04630896 |
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| Source dataset | uspto-grants-1986_12 |
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| ORD ID | ord-2f72dcc3ed3b40bbbac204edef6a2d0e |
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| Source note | uspto-grants-1986_12 |
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