HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 2-Chloro-4,6-dimethyl-3-pyridinecarbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 3-Cyano-4,6-dimethyl-2-hydroxypyridine | HCID 69856 | — |
| Product | 2-Chloro-4,6-dimethyl-3-pyridinecarbonitrile | HCID 223261 | — |
Reaction Steps
2-Chloro-3-cyano-4,6-dimethylpyridine was prepared from 3-cyano-4,6-dimethylpyrid-2-one and phosphorus oxychloride following the procedure of Kametani and Sato (Yakugaka Kenyu 34, 117, 1962).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04631081 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-5b6600c3d1f7466e858e9a3af8f1837b |
| Source note | uspto-grants-1986_12 |