HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isotridecan-1-ol → 1,2,3,4,5-Pentaisotridecyloxycarbonylcyclopentadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isotridecan-1-ol | HCID 33865 | — |
| Reactant | Pentamethyl cyclopentadiene-1,2,3,4,5-pentacarboxylate | HCID 494485 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1,2,3,4,5-Pentaisotridecyloxycarbonylcyclopentadiene | HCID 20155084 | 100.2% |
Reaction Steps
7.13 g (20 mmol) of 1,2,3,4,5-pentamethoxycarbonylcyclopentadiene are treated with 20.0 g (100 mmol) of isotridecyl alcohol. 3.12 g (97.5% of the theoretical yield) of methanol are distilled off at 100° C. within 8 h, firstly at 1013 mbar, then at from 363 to 18 mbar. 24 g of 1,2,3,4,5-pentaisotridecyloxycarbonylcyclopentadiene are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04631243 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-06999c9c110c4195ad4f0e20ffd54137 |
| Source note | uspto-grants-1986_12 |