Methyl Bromide → HCID 13590776, compound

HRID 1249353Notes

Reaction equation

HRID 1249353 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][O:9][CH:10]2[CH:15]3[O:16][C:17]4[CH:23]=[CH:22][CH:21]=[C:20]([O:24][CH3:25])[C:18]=4[O:19][CH:14]3[CH2:13][CH2:12][CH2:11]2)[CH2:3][CH2:2]1.[CH3:26][Br:27]>>[Br-:27].[CH3:25][O:24][C:20]1[C:18]2[O:19][CH:14]3[CH2:13][CH2:12][CH2:11][CH:10]([O:9][CH2:8][CH2:7][N+:4]4([CH3:26])[CH2:5][CH2:6][O:1][CH2:2][CH2:3]4)[CH:15]3[O:16][C:17]=2[CH:23]=[CH:22][CH:21]=1

Participants

3

Reactant 2

HCID 6323Methyl BromideHCID 13590770HCID 13590770, compound

Product 1

HCID 13590776HCID 13590776, compound

Procedure

Following the same procedure as in Example 8, 3.5 g (0.01 mole) of the amino ether of Example 4 were used at the start to obtain, after the action of methyl bromide, 3.3 g of the title-product of melting point 167.1° C., having the elementary analysis:

Workup

  1. customto obtain

Sources & evidence

ORD record
ord-96df9653187a42798044a617d502b084
Source dataset
uspto-grants-1986_12
Patent number
US04631277

Reaction notes

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