Water → HCID 6404487, compound

HRID 1249355Notes

Reaction equation

HRID 1249355 reaction equation
[C:1]1([C:7]2[CH:8]=[C:9]([C:14]([NH2:16])=O)[C:10](=O)[NH:11][N:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.O.P(Cl)(Cl)([Cl:20])=O>>[Cl:20][C:10]1[N:11]=[N:12][C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[CH:8][C:9]=1[C:14]#[N:16]

Participants

4

Reactant 3

HCID 962WaterHCID 24813Phosphorus oxychlorideHCID 14753284D-083

Product 1

HCID 6404487HCID 6404487, compound

Conditions

Temperature
80 °C

Procedure

1.5 g of the product obtained in Example 1 are dissolved in 20 ml of phosphorus oxychloride and the solution is then heated at 80° C. for 5 hours. The mixture is poured into 50 ml of water. A precipitate appears, which is filtered off and dried.

Workup

  1. filtrationwhich is filtered off
  2. customdried

Sources & evidence

ORD record
ord-45aee8a62c7e47e183b152d6f3fd8abb
Source dataset
uspto-grants-1986_12
Patent number
US04631280

Reaction notes

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