HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenoxyacetic Acid → Phenoxyacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenoxyacetic Acid | HCID 19188 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Phenoxyacetyl chloride | HCID 69703 | — |
Reaction Steps
Phenoxyacetic acid (d5) was treated with 25 ml of thionyl chloride and stirred for 18 hours at room temperature. After the end of the reaction, the reaction mixture was concentrated under vacuum at 30° C. to provide phenoxyacetyl chloride (4.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06334997B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-92b52fe2c1d64758b0993ba7f1a2bf6e |
| Source note | uspto-grants-2002_01 |