3-Amino-1,2-propanediol → HCID 15847428, compound

HRID 1249659Notes

Reaction equation

HRID 1249659 reaction equation
[NH2:1][CH2:2][CH:3]([OH:6])[CH2:4][OH:5].[CH2:7]([NH:19][C:20](N1C=CN=C1)=[O:21])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>CO>[OH:6][CH:3]([CH2:4][OH:5])[CH2:2][NH:1][C:20]([NH:19][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:21]

Participants

4

Reactant 2

HCID 735613-Amino-1,2-propanediolHCID 18328494HCID 18328494, compound

Product 1

HCID 15847428HCID 15847428, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The preparation was carried out, according to the same process described in Example 1, from 2.3 g of 3-amino-1,2-propanediol of corresponding formula R2—NH—R3, where R2 denoted H and R3 denoted —CH2—CHOH—CH2OH, and 7 g of 1-N-(dodecylaminocarbonyl)imidazole of corresponding formula (II), where R1 denoted C12H25, in 100 cm3 of methanol.

Sources & evidence

ORD record
ord-36b3ac33faf646719ec04f93742dbc33
Source dataset
uspto-grants-2002_01
Patent number
US06335024B2

Reaction notes

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