HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 22495826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 22495894 | HCID 22495894 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22495826 | HCID 22495826 | — |
Reaction Steps
120.00 g (0.33 mol) of 4-(5-chloro-2-nitro-benzoylamino)-benzenesulfonyl fluoride, 29.10 g (0.33 mol) of morpholine and 33.85 g (0.33 mol) of triethylamine were stirred in 1200 ml of toluene at 60° C. for 2 days. The precipitated solid was filtered off with suction and recrystallized from acetone/n-hexane. 102.10 g (71%) of the title compound having a melting point of 243-245° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06335334B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-7f35f79445954fec89a44f7a4da77281 |
| Source note | uspto-grants-2002_01 |