HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylene Glycol → L-lactide epsilon-caprolactone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylene Glycol | HCID 1030 | — |
| Solvent | 1,1,1,3,3,3-Hexafluoro-2-propanol | HCID 13529 | — |
| Product | L-lactide epsilon-caprolactone | HCID 131710947 | — |
Reaction Steps
The procedure in Example 3 was substantially repeated, except that 4.4 mL (60 mmol) propylene glycol (USP grade) was used instead of 5.6 mL of 1-dodecanol. The copolymer had an inherent viscosity of 0.17 dL/g in HFIP at 25° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06335383B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-87ea280ad50d4b1587b21ad9997b7792 |
| Source note | uspto-grants-2002_01 |