HuagongsheHuagongshe Chemistry Print Report · For research reference only
Magnesium → HCID 18329057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Magnesium | HCID 5462224 | — |
| Reactant | HCID 54110016 | HCID 54110016 | — |
| Product | HCID 18329057 | HCID 18329057 | — |
Reaction Steps
This compound was prepared from 4,5-methylenedioxyindole-2-carboxylic acid methyl ester as described in example 1. However this time 10 equivalence of magnesium turnings were used instead of 2-3 eq. of magnesium turnings. The product was purified by column chromatography on silica gel using 7:3 petroleum spirit:ethyl acetate as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06335360B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-2a88eaa187644befbdeaaaffce7f7bd5 |
| Source note | uspto-grants-2002_01 |