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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1250107Generated: November 1, 2026

Potassium Carbonate → HCID 53979024, compound

https://huagongshe.com/reaction/1250107

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactanttert-Butyl bromoacetateHCID 79177—
Reactant3-Bromo-2-methylphenolHCID 11171430—
SolventAcetoneHCID 180—
ProductHCID 53979024HCID 53979024101.7%

Reaction Steps

Tert-butyl bromoacetate (1.08 mL, 7.27 mmol) and potassium carbonate (2.01 g, 14.55 mmol) were added to a solution of 3-bromo-2-methylphenol (1.29 g, 6.92 mmol) in acetone (17 mL), and the mixture was stirred at room temperature for 5 hours under a nitrogen atmosphere. The mixture was filtered, and the filtrate was evaporated to dryness to give (3-bromo-2-methylphenoxy)acetic acid tert-butyl ester as a pale yellow oil (2.12 g, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06335459B1
Source datasetuspto-grants-2002_01
ORD IDord-51c7ec62948f4cfbb44bc4ab0116571d
Source noteuspto-grants-2002_01