HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 53979024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | 3-Bromo-2-methylphenol | HCID 11171430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 53979024 | HCID 53979024 | 101.7% |
Reaction Steps
Tert-butyl bromoacetate (1.08 mL, 7.27 mmol) and potassium carbonate (2.01 g, 14.55 mmol) were added to a solution of 3-bromo-2-methylphenol (1.29 g, 6.92 mmol) in acetone (17 mL), and the mixture was stirred at room temperature for 5 hours under a nitrogen atmosphere. The mixture was filtered, and the filtrate was evaporated to dryness to give (3-bromo-2-methylphenoxy)acetic acid tert-butyl ester as a pale yellow oil (2.12 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06335459B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-51c7ec62948f4cfbb44bc4ab0116571d |
| Source note | uspto-grants-2002_01 |