Benzenamine, 3,5-bis(trifluoromethyl)- → HCID 18328565, compound

Participants

Reaction Steps

Into a 250 mnL Schlenk vessel was placed 100 mL of dry TBF, 3.50 g of oxalyl chloride and 12.4 g of 3,5-bis(trifluoromethyl)aniline. The mixture was refluxed under argon for 12 hours and then allowed to cool. All of the solvent was removed in vacuo to leave a pale brown solid. This was washed with hexane and toluene and pumped dry. Yield 10.33 g.

Provenance & Evidence