HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → HCID 18327504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Product | HCID 18327504 | HCID 18327504 | — |
Reaction Steps
The 2-chloro4-(4-methoxyphenylsulphanyl)pyrimidine was prepared in a similar manner to the analogous starting material of Example 1, from 4-methoxybenzenethiol (1.90 g, 13.4 mmol), 2,4-dichloropyrimidine (2.0 g, 13.4 mmol) and sodium hydride [60% dispersion in oil] (590 mg, 14.8 mmol) as an off-white solid m.p. 69-70°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06337335B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-7db01ccdb16e4af0b532497b6e4e7098 |
| Source note | uspto-grants-2002_01 |