HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 9840386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 11058459 | HCID 11058459 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9840386 | HCID 9840386 | 94% |
Reaction Steps
The sub-title product of step c) (0.17 g, 0.44 mmol) was dissolved in THF (3 ml) and aqueous methyl amine (40%, 3 ml) and stirred for 30 minutes. The solvent was removed and the product precipitated from diethyl ether to give the title compound (0.14 g, 94%) as a slightly brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06337342B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-5c7d6d6cba174aa98bf1f687bc51a3ed |
| Source note | uspto-grants-2002_01 |