HCID 45118278, compound → HCID 18327317, compound

HRID 1250229Notes

Reaction equation

HRID 1250229 reaction equation
C(OC([N:8]1[CH2:13][CH2:12][CH:11]([CH2:14][CH2:15][CH2:16][N:17]2[C:26](=[O:27])[C:25]3[C:20](=[C:21]([O:28][CH3:29])[CH:22]=[CH:23][CH:24]=3)[N:19]=[C:18]2[CH3:30])[CH2:10][CH2:9]1)=O)(C)(C)C>Cl.CCO>[CH3:29][O:28][C:21]1[CH:22]=[CH:23][CH:24]=[C:25]2[C:20]=1[N:19]=[C:18]([CH3:30])[N:17]([CH2:16][CH2:15][CH2:14][CH:11]1[CH2:10][CH2:9][NH:8][CH2:13][CH2:12]1)[C:26]2=[O:27]

Participants

3

Reactant 1

HCID 45118278HCID 45118278, compound

Product 1

HCID 18327317HCID 18327317, compound

Reagents, catalysts & solvents 1

HCID 21887872Ethanol hydrochlorideSolvent

Procedure

The product from Step A above was dissolved in conc HCl/EtOH (1:2 mixture, 18 mL) and was stirred for 1 h. The reaction mixture was concentrated under vacuum and azeoptroped with EtOH (2×) to provide the desired product as a white solid. API-MS: 316 (M+1)

Workup

  1. concentrationThe reaction mixture was concentrated under vacuum and azeoptroped with EtOH (2×)

Sources & evidence

ORD record
ord-55c32d83f6a34c3baebcb08af70c3dd6
Source dataset
uspto-grants-2002_01
Patent number
US06337332B1

Reaction notes

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