HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 45118278, compound → HCID 18327317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 45118278 | HCID 45118278 | — |
| Solvent | Ethanol hydrochloride | HCID 21887872 | — |
| Product | HCID 18327317 | HCID 18327317 | — |
Reaction Steps
The product from Step A above was dissolved in conc HCl/EtOH (1:2 mixture, 18 mL) and was stirred for 1 h. The reaction mixture was concentrated under vacuum and azeoptroped with EtOH (2×) to provide the desired product as a white solid. API-MS: 316 (M+1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06337332B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-55c32d83f6a34c3baebcb08af70c3dd6 |
| Source note | uspto-grants-2002_01 |