HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 18327890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Triphenylphosphine Oxide | HCID 13097 | — |
| Reactant | HCID 18327893 | HCID 18327893 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18327890 | HCID 18327890 | — |
Reaction Steps
The sub-title compound was prepared according to the method described in Example 1(ii) above from 1.4 g (8.1 mmol) of 4-azidomethyl-3-methylbenzonitrile (from step (iv) above) and 2.3 g (9.0 mmol) of triphenylphosphine in 18 mL of ethanol and 2 mL of water. Yield: 0.60 g (contaminated by triphenylphosphine oxide; estimated actual yield: 0.36 g (28%)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06337394B2 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-adf0e9e5fcc44282abfc735fd0a15dc7 |
| Source note | uspto-grants-2002_01 |