HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 15480187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | 1-(4-Phenoxyphenyl)-1H-imidazole | HCID 18326638 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 15480187 | HCID 15480187 | — |
Reaction Steps
137 mmol of 1-(4-phenoxyphenyl)imidazole are dissolved in 250 ml of chloroform. 190 mmol of chlorosulphonic acid are then added dropwise. The whole is left at 45° C. overnight. After cooling and removal of the solvent by evaporation, the resulting oil is taken up in diethyl ether. The resulting solid is filtered off and dried to yield the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06339092B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-fabf148c68754a6dbcbf2d6965c22220 |
| Source note | uspto-grants-2002_01 |