HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → 2,4-Diallylamino-6-nitroquinazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 4-Allylamino-2-chloro-6-nitroquinazoline | HCID 18326487 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,4-Diallylamino-6-nitroquinazoline | HCID 57117446 | 80.6% |
Reaction Steps
A mixture of 265 mg (1.00 mmol) of 4-allylamino-2-chloro-6-nitroquinazoline and 1.52 g (26.65 mmol) of allylamine were stirred at room temperature for 2.5 hours. Water was added to the reaction mixture, and crystals thus precipitated were filtered out to give 230 mg (yield: 80.6%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06339089B2 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-d1ab6a985b6c42d8843a992088c45bf1 |
| Source note | uspto-grants-2002_01 |