HRID1250557

反应详情

EQUATION

反应方程式

HRID 1250557 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 265 mg (1.00 mmol) of 4-allylamino-2-chloro-6-nitroquinazoline and 1.52 g (26.65 mmol) of allylamine were stirred at room temperature for 2.5 hours. Water was added to the reaction mixture, and crystals thus precipitated were filtered out to give 230 mg (yield: 80.6%) of the title compound.

WORKUP

后处理

  1. customthus precipitated
  2. filtrationwere filtered out