HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 18326565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 4-Allylamino-2-chloro-6-nitroquinazoline | HCID 18326487 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18326565 | HCID 18326565 | 99.4% |
Reaction Steps
A mixture of 250 mg (0.95 mmol) of 4-allylamino-2-chloro-6-nitroquinazoline and 694 mg (11.74 mmol) of isopropylamine was stirred at room temperature for 3 hours. Water was added to the reaction mixture, and crystals thus precipitated were filtered to give 270 mg (yield: 99.4%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06339089B2 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-bdcb88a2e8f64ef3857dde83a8e68125 |
| Source note | uspto-grants-2002_01 |