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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1250771Generated: November 1, 2026

HCID 9894515, compound → HCID 18520283, compound

https://huagongshe.com/reaction/1250771

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9894515HCID 9894515—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
SolventEthyl AcetateHCID 8857—
ProductHCID 18520283HCID 18520283—

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (1.2 ml) was added to a solution containing N-(3-morpholinopropyl)-3-[2-(octadecyloxy)phenyl]propanamide (1.88 g) in ethyl acetate (38 ml) at room temperature. After being stirred for 45 minutes, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-ethanol, thereby yielding the entitled compound (1.89 g) as white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06339154B1
Source datasetuspto-grants-2002_01
ORD IDord-3bc399051a0c47718bcf8bc591994e11
Source noteuspto-grants-2002_01