HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenylboronic acid → HCID 18325035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenylboronic acid | HCID 285645 | — |
| Reactant | 4-(Trifluoromethyl)phenylboronic acid | HCID 2734389 | — |
| Reactant | HCID 18324985 | HCID 18324985 | — |
| Product | HCID 18325035 | HCID 18325035 | — |
Reaction Steps
Following the procedure of Example 1, Step 5, but substituting 3-bromo-2-(4-(methylthio)phenyl)-4H-1-benzopyran-4-one(0.1 g, 0.32 mmol) for 3-iodo-2-(4-(methylsulfonyl)phenyl)-4H-1-benzopyran-4-one and 4-trifluoromethylbenzeneboronic acid(0.066 g, 0.35 mmol) for 4-fluorobenzeneboronic acid, the title compound was obtained as a solid(0.05 g, 40%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06340694B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-da85734d8aaa4ccfa4642b715a10987d |
| Source note | uspto-grants-2002_01 |