HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-butyne → HCID 11337003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-butyne | HCID 2756862 | — |
| Reactant | HCID 11150633 | HCID 11150633 | — |
| Product | HCID 11337003 | HCID 11337003 | — |
Reaction Steps
2-(4-But-2-ynyloxy-phenylsulfanyl)-octanoic acid ethyl ester was prepared according to the general method as outlined in Example 1 (Step 2). Starting from 2-(4-hydroxy-phenylsulfanyl)-octanoic acid ethyl ester 13.6 g, 46 mmol) and 1-bromo-2-butyne(6.23 g, 47mmol). Yield 13.78 g (86%); amber oil; MS: 349.0 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06340691B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-05c0b84e026b4e4ab8707dfee4704418 |
| Source note | uspto-grants-2002_01 |